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Tuesday, August 13, 2013

Isolation and Characterization of Eugenol Form Cloves

Title: Experiment 1- closing off & Characterisation of Eugenol from split trees Objectives: 1. To seize eugenol and other quicksilver(a) natural products from splits by go distillment 2. To restrict eugenol by bollocks chromatography-mass spectroscopy (GC-MS) and IR spectroscopy. debut: clove tree vegetable crude oil is an essential oil extracted from the clove plant, Syzygium aromaticum or genus Eugenia caryophyllate and Eugenia aomaticum. There be only minute differences amongst these species and many consider them to be essentially the same. The clove oil has only three memorise components: eugenol, acetyleugenol or eugenol acetate, and ?-caryophyllene. In this experiment, eugenol is isolate from ground cloves by locomote distillate and is identify by infrared spectroscopy and bollocks chromatography-mass spectroscopy (GC-MS). Eugenol is acerb because of the phenol group. It has many medical properties, particularly as a distressingness killer and aid to digestion, and is employ widely in toothpaste and dental preparations. Eugenol acetate is a caseful of ester. It is used as scent and flavorings. Caryophyllene is a hydrocarbon that belongs to the family of sesquiterpenes. Eugenol acetate and caryophyllene are natural products and basis be separated from eugenol through acid-base extraction.
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The bodily structure of the three major components contained in clove oil is shown below. figure 1.0- Eugenol Figure 2.0-Eugenol acetate Figure 3.0- ?-caryophyllene use: Isolation of the Essential cover: 1. About 10g of sweet-scented cloves (stored in a closed container) is burden and a mortar and postage stamp is used to grind them. 2. The pulverize is transferred to a 500mL distillation flask and 200mL of distilled pee is added.A simple distillation apparatus is assembled as shown. If available, waxy clips are used. 3. In a 100mL round rat flask, 60mL of water is poured and the level of the liquid is tag with a scratch or tape. The water is poured out and this flask is used as the...If you extremity to get a wide-eyed essay, order it on our website: Orderessay

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